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sciencemadness discussion board preparation of white phosphorus via reduction

Preparation of elemental phosphorus - ScienceMadness.org

May 6, 2012 ... However all of this is being done through my own lens so to speak and .... They produced white-bright little flames, so I guess some phosphorus got lost in that way. ... I have, a couple of times, tried straightforward phosphate reduction with ..... The forum has seen much discussion regarding phosphides and...

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Sciencemadness Discussion Board - RDX synthesis - Powered by XMB 1 ...

when i come back, there are short white fibers and no liquid. i dont think it's .... whether it's possible to prepare RDX using HNO3/P2O5 as a nitrating agent. ... dinitrate puts some HNO3, so one may decrease amount of conc HNO3). .... and you will start to see white phosphorus form in the bottom of the flask,...

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Phenylalanine to amphetamine or N-methylamphetamine - The Vespiary

The first method uses Lithium Aluminium Hydride to reduce ... Now obviously those are not OTC, and require multi-step synthesis using some nasty chems. ... reducing phenylalaninol to amphetamine with 80% yields using phosphorous acid ... A highly regarded member also wrote this at science madness,...

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Making Potassium Chlorate - Metal Lab

Apr 23, 2012 ... Note: These experiments are performed over 10 years ago (end of 2000). ... With Phosphorus or even sulphur in may ignite easily. ... water, compared to sodium chlorate and chlorides, it is to prepare rather purely. ... An extensive discussion on this subject (MMO anodes) is on the Sciencemadness forum.

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Preparation of elemental phosphorus - ScienceMadness.org

May 6, 2012 ... However all of this is being done through my own lens so to speak and .... They produced white-bright little flames, so I guess some phosphorus got lost in that way. ... I have, a couple of times, tried straightforward phosphate reduction with ..... The forum has seen much discussion regarding phosphides and...

More details » Get Price

Sciencemadness Discussion Board - RDX synthesis - Powered by XMB 1 ...

when i come back, there are short white fibers and no liquid. i dont think it's .... whether it's possible to prepare RDX using HNO3/P2O5 as a nitrating agent. ... dinitrate puts some HNO3, so one may decrease amount of conc HNO3). .... and you will start to see white phosphorus form in the bottom of the flask,...

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Science & Chemistry - 420chan

420chan Discussion .... Was trying to remember an awesome home mad science forum I ... Also, its landing page had an alchemist-style seal on a white background. ... Do future energy demands need to be reduced for us to survive as a .... I think that the phosphorus pentoxide (P2O5) with NaCl route might...

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Current Projects - Bromic Acid

Phosphorus ... Preparation of THF using OTC Pentoses as the starting material. ... reduce any aluminate formed via the heat of the initial thermite like reaction. ..... (by Esplosivo from the sciencemadness discussion board), the reaction between...

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Sciencemadness Discussion Board - RDX synthesis - Powered by XMB 1 ...

when i come back, there are short white fibers and no liquid. i dont think it's .... whether it's possible to prepare RDX using HNO3/P2O5 as a nitrating agent. ... dinitrate puts some HNO3, so one may decrease amount of conc HNO3). .... and you will start to see white phosphorus form in the bottom of the flask,...

More details » Get Price

Phenylalanine to amphetamine or N-methylamphetamine - The Vespiary

The first method uses Lithium Aluminium Hydride to reduce ... Now obviously those are not OTC, and require multi-step synthesis using some nasty chems. ... reducing phenylalaninol to amphetamine with 80% yields using phosphorous acid ... A highly regarded member also wrote this at science madness,...

More details » Get Price

Making Potassium Chlorate - Metal Lab

Apr 23, 2012 ... Note: These experiments are performed over 10 years ago (end of 2000). ... With Phosphorus or even sulphur in may ignite easily. ... water, compared to sodium chlorate and chlorides, it is to prepare rather purely. ... An extensive discussion on this subject (MMO anodes) is on the Sciencemadness forum.

More details » Get Price

Sean Breheny - YouTube

In this video we make a small amount of Carbon disulfide using a ceramic tube and a very hot torch. ... Next video is to be posted is synthesis of BROMINE! .... This procedure was taken from the ScienceMadness forum: ..... I dissolved about 600mg of the white allotrope of phosphorus in about 6mL carbon disulfide. I then put...

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Sciencemadness Discussion Board - RDX synthesis - Powered by XMB 1 ...

when i come back, there are short white fibers and no liquid. i dont think it's .... whether it's possible to prepare RDX using HNO3/P2O5 as a nitrating agent. ... dinitrate puts some HNO3, so one may decrease amount of conc HNO3). .... and you will start to see white phosphorus form in the bottom of the flask,...

More details » Get Price

Making Potassium Chlorate - Metal Lab

Apr 23, 2012 ... Note: These experiments are performed over 10 years ago (end of 2000). ... With Phosphorus or even sulphur in may ignite easily. ... water, compared to sodium chlorate and chlorides, it is to prepare rather purely. ... An extensive discussion on this subject (MMO anodes) is on the Sciencemadness forum.

More details » Get Price

Science & Chemistry - 420chan

420chan Discussion .... Was trying to remember an awesome home mad science forum I ... Also, its landing page had an alchemist-style seal on a white background. ... Do future energy demands need to be reduced for us to survive as a .... I think that the phosphorus pentoxide (P2O5) with NaCl route might...

More details » Get Price

Current Projects - Bromic Acid

Phosphorus ... Preparation of THF using OTC Pentoses as the starting material. ... reduce any aluminate formed via the heat of the initial thermite like reaction. ..... (by Esplosivo from the sciencemadness discussion board), the reaction between...

More details » Get Price

Sciencemadness Discussion Board - RDX synthesis - Powered by XMB 1 ...

when i come back, there are short white fibers and no liquid. i dont think it's .... whether it's possible to prepare RDX using HNO3/P2O5 as a nitrating agent. ... dinitrate puts some HNO3, so one may decrease amount of conc HNO3). .... and you will start to see white phosphorus form in the bottom of the flask,...

More details » Get Price

Sciencemadness Discussion Board - Anthranilic Acid Synthesis ...

Sciencemadness Discussion Board ... Anthranilic Acid Synthesis ... selectively nitrate benzoic acid on the meta position and then reduce it to an amine in the .... It's funny/strange that red phosphorus is near impossible to buy (for individuals) but methyl anthranilate is sold in bulk quantities over the counter.

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Current Projects - Bromic Acid

Phosphorus ... Preparation of THF using OTC Pentoses as the starting material. ... reduce any aluminate formed via the heat of the initial thermite like reaction. ..... (by Esplosivo from the sciencemadness discussion board), the reaction between...

More details » Get Price

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